RT Journal Article T1 Manufacturing of hemicellulosic oligosaccharides from fast-growing Paulownia wood via autohydrolysis: Microwave versus conventional heating A1 Garcia Del Rio, Pablo A1 Perez Perez, Alba A1 Garrote Velasco, Gil A1 Gullon Estevez, Beatriz K1 3303.03 Procesos Químicos K1 2403 Bioquímica AB Microwave hydrothermal treatment (MHT) is considered a sustainable technology for the valorization of lignocellulosic materials, enabling the solubilization of hemicellulosic-derived compounds, especially in the form of oligosaccharides that may present potential in the chemical, pharmaceutical or nutraceutical industries. Hence, MHT at 200 and 230 °C, at severity (S0) among 2.92–4.66 were performed. S0 = 3.98 permitted the recovery of about 80% of the initial xylan as xylooligosaccharides. In order to compare the effectiveness of MHT, conventional hydrothermal treatment (CHT) was performed at conditions leading to the maximum recovery of oligosaccharides (S0 =3.98, non-isothermal regime at 203 °C). Despite the structural features of oligomers in the three liquors were very similar, the spent solids presented different enzymatic digestibility, which implied a different effect of the treatments, reaching up to 80% of glucan to glucose conversion for the solid after MHT at 230 °C for 0.5 min. Additionally, CHT consumed 2.1–2.8-fold greater energy than MHT, reflecting that microwave-assisted autohydrolysis is a sustainable and efficient technology to process PW. PB Industrial Crops and Products SN 09266690 YR 2022 FD 2022-11 LK http://hdl.handle.net/11093/3726 UL http://hdl.handle.net/11093/3726 LA eng NO Industrial Crops and Products, 187, 115313 (2022) NO Financiado para publicación en acceso aberto: Universidade de Vigo/CISUG NO Agencia Estatal de Investigación | Ref. PID2019-110031RB-I00 DS Investigo RD 04-dic-2024